化工社化工社 化学情報印刷レポート · 研究参考用
Cyclohexanone → 1,5-Dioxaspiro[5.5]undec-3-ylmethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexanone | HCID 7967 | — |
| 反応物 | Trimethylolmethane | HCID 78432 | — |
| 生成物 | 1,5-Dioxaspiro[5.5]undec-3-ylmethanol | HCID 15286693 | 65% |
反応手順
The same procedure as in the step (1a) of Example 1 was repeated using 2-(hydroxymethyl)-1,3-propanediol and cyclohexanone to obtain the title compound (2.26 g, yield: 65%) as a light yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07425634B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-5cb5e6131adb45fb800cd2a1b6dcb053 |
| 出典メモ | uspto-grants-2008_09 |