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Ethyl Acetoacetate → 2-(2,5,5-Trimethyl-1,3-dioxan-2-yl)ethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Acetoacetate | HCID 8868 | — |
| 反応物 | Neopentyl glycol | HCID 31344 | — |
| 反応物 | 2-(2-Propyl-1,3-dioxan-2-yl)ethanol | HCID 59792435 | — |
| 生成物 | 2-(2,5,5-Trimethyl-1,3-dioxan-2-yl)ethanol | HCID 23252950 | 55% |
反応手順
The same procedure as in the steps (8a) and (8b) of Example 8 was repeated using ethyl acetoacetate, and 2,2-dimethyl-1,3-propanediol to obtain the title compound (7.3 g, total yield: 55%) as a light yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07425634B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-3eddc8993b914b09824dff92265f7283 |
| 出典メモ | uspto-grants-2008_09 |