化工社化工社 化学情報印刷レポート · 研究参考用
Cyanocyclobutane → (1-Cyclobutyl-2,6,7-trioxabicyclo[2.2.2]oct-4-yl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyanocyclobutane | HCID 78148 | — |
| 反応物 | (1-Cyclopropyl-2,6,7-trioxabicyclo[2.2.2]oct-4-yl)methanol | HCID 59792605 | — |
| 生成物 | (1-Cyclobutyl-2,6,7-trioxabicyclo[2.2.2]oct-4-yl)methanol | HCID 59792382 | 51% |
反応手順
The same procedure as in the steps (37a) to (37c) of Example 37 was repeated using cyclobutanecarbonitrile to obtain the title compound (15 g, total yield: 51%) as a light yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07425634B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-8161260e18284c7b83865735b591d5c1 |
| 出典メモ | uspto-grants-2008_09 |