化工社化工社 化学情報印刷レポート · 研究参考用
2-Imidazoline → 1-(4-Ethylphenyl)-2-imidazolylethan-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Imidazoline | HCID 68156 | — |
| 反応物 | 2-Bromo-1-(4-ethylphenyl)ethan-1-one | HCID 12401951 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 1-(4-Ethylphenyl)-2-imidazolylethan-1-one | HCID 22142578 | — |
反応手順
1 mmol of 2-bromo-1-(4-ethylphenyl)ethan-1-one in acetonitrile was added drop wise to 5.5 mmol imidazoline in acetonitrile at room temperature for fourteen hours. The reaction mixture was concentrated in vacuo and diluted with water and ethyl acetate. The solution was extracted three times with ethyl acetate and dried over sodium sulfate to obtain 1-(4-ethylphenyl)-2-imidazolylethan-1-one.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07425557B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-24ee89c2f0684d92a2fe9090065cfceb |
| 出典メモ | uspto-grants-2008_09 |