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HRID 31779作成日:2026年10月25日

2-Imidazoline → 1-(4-Ethylphenyl)-2-imidazolylethan-1-one

https://huagongshe.com/reaction/31779

反応式

関与物質

役割名称HCID仕込み量
反応物2-ImidazolineHCID 68156—
反応物2-Bromo-1-(4-ethylphenyl)ethan-1-oneHCID 12401951—
溶媒AcetonitrileHCID 6342—
生成物1-(4-Ethylphenyl)-2-imidazolylethan-1-oneHCID 22142578—

反応手順

1 mmol of 2-bromo-1-(4-ethylphenyl)ethan-1-one in acetonitrile was added drop wise to 5.5 mmol imidazoline in acetonitrile at room temperature for fourteen hours. The reaction mixture was concentrated in vacuo and diluted with water and ethyl acetate. The solution was extracted three times with ethyl acetate and dried over sodium sulfate to obtain 1-(4-ethylphenyl)-2-imidazolylethan-1-one.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07425557B2
出典データセットuspto-grants-2008_09
ORD IDord-24ee89c2f0684d92a2fe9090065cfceb
出典メモuspto-grants-2008_09