化工社化工社 化学情報印刷レポート · 研究参考用
2-Pyridineethanamine → 2-aminopyrido[2,3-d]pyrimidin-7(8H)-one 36
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Pyridineethanamine | HCID 75919 | — |
| 反応物 | 6-(2,6-Dichlorophenyl)-8-methyl-2-(methylthio)pyrido[2,3-d]pyrimidin-7(8H)-one | HCID 10736701 | — |
| 生成物 | 2-aminopyrido[2,3-d]pyrimidin-7(8H)-one 36 | HCID 5327883 | — |
反応手順
This compound was prepared by a procedure similar to that described in Example 49 starting with 0.165 g (0.47 mmol) of 6-(2,6-dichlorophenyl)-8-methyl-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one of Example 37 and 1.00 g (8.20 mmol) of 2-(2-aminoethyl)-pyridine yielding 0.082 g of pure product; mp 173°-174° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05733914 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-3a132906f38a4c07b3d4eb7a38743313 |
| 出典メモ | uspto-grants-1998_03 |