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1-(4,4-Dimethylcyclohex-1-enyl)-2-nitrobenzene → 2-(4,4-Dimethylcyclohexyl)aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(4,4-Dimethylcyclohex-1-enyl)-2-nitrobenzene | HCID 23142003 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | 2-(4,4-Dimethylcyclohexyl)aniline | HCID 15340111 | — |
反応手順
A mixture of 1-(4,4-dimethylcyclohex-1-enyl)-2-nitrobenzene (16.3 g, 70.5 mmol) prepared in Example (3a), 10% palladium on carbon (1 g, wet) and ethyl acetate (100 mL) was stirred for 14 hours and 30 minutes under a hydrogen atmosphere at atmospheric pressure and room temperature.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07425554B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-10fe35a6694f4bad8e1553d8d6b3a1f6 |
| 出典メモ | uspto-grants-2008_09 |