化工社化工社 化学情報印刷レポート · 研究参考用
Oxalyl chloride → 2,3-Dichloro-6-iodobenzoic acid chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 反応物 | 2,3-Dichloro-6-iodobenzoic acid | HCID 22008816 | — |
| 触媒 | Dimethylformamide | HCID 6228 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | 2,3-Dichloro-6-iodobenzoic acid chloride | HCID 54292031 | — |
反応手順
DMF (one drop) was added to a stirred solution of 2,3-dichloro-6-iodobenzoic acid (1.53 g, 4.83 mmol) and oxalyl chloride (2 ml) in ethyl acetate (20 ml). After 2 hours, the solution was evaporated and the product was used immediately.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06211189B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-7726a461dd284d93b0a1fcdd654e9b25 |
| 出典メモ | uspto-grants-2001_04 |