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HRID 322008作成日:2026年10月25日

Nitric Acid → 2,6-Dimethyl-3-nitrobenzoic acid

https://huagongshe.com/reaction/322008

反応式

関与物質

役割名称HCID仕込み量
反応物Nitric AcidHCID 944—
反応物Sulfuric AcidHCID 1118—
反応物2,6-Dimethylbenzoic acidHCID 12439—
生成物2,6-Dimethyl-3-nitrobenzoic acidHCID 239329—

反応条件

温度0 °C

反応手順

13.5 g (90.0 mmol) of 2,6-dimethylbenzoic acid were introduced in portions into a solution of 25 ml of conc. sulfuric acid and 25 ml of 65% strength HNO3 cooled to 0° C. After stirring at 0° C. for 1 h, the reaction mixture was poured onto ice, and the precipitate deposited was filtered off with suction and dried. 15.5 g of the title compound resulted.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06211196B1
出典データセットuspto-grants-2001_04
ORD IDord-790e5437b9c847eaaa58a676fb399b9e
出典メモuspto-grants-2001_04