化工社化工社 化学情報印刷レポート · 研究参考用
2-(Benzyloxy)benzaldehyde → HCID 22009001、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Benzyloxy)benzaldehyde | HCID 344784 | — |
| 反応物 | HCID 178418507 | HCID 178418507 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | HCID 22009001 | HCID 22009001 | — |
反応手順
2-(benzyloxy)benzaldehyde (5g, 23.6 mmol) was reacted with vinylmagnesium bromide in THF (90 ml) at 0 C. The reaction was quenched with 2 N HCl and the product was extracted in i-PrOAc, dried over Na2SO4 and purified by flash chromatography with EtOAc:toluene 2.5:97.5.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06211197B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-a4708b1709d247f8a0d9098dd75df039 |
| 出典メモ | uspto-grants-2001_04 |