Methanesulfonyl chloride → 3-(3-Chloro-4-methoxymethoxyphenyl)propyl methanesulfonate
反応式
[Cl:1][C:2]1[CH:3]=[C:4]([CH2:12][CH2:13][CH2:14][OH:15])[CH:5]=[CH:6][C:7]=1[O:8][CH2:9][O:10][CH3:11].[CH3:16][S:17](Cl)(=[O:19])=[O:18]>>[CH3:16][S:17]([O:15][CH2:14][CH2:13][CH2:12][C:4]1[CH:5]=[CH:6][C:7]([O:8][CH2:9][O:10][CH3:11])=[C:2]([Cl:1])[CH:3]=1)(=[O:19])=[O:18]参加物
3
実験手順
In substantially the same manner as in Reference Example 85, 3-(3-chloro-4-methoxymethoxyphenyl)propanol was reacted with methanesulfonyl chloride to obtain 3-(3-chloro-4-methoxymethoxyphenyl)propyl methanesulfonate as an oil. The yield was quantitative.
出典と根拠
- ORDレコード
- ord-58565da7849d48b58894f9d852c8a9c9
- 出典データセット
- uspto-grants-2001_04
- 特許番号
- US06211215B1
反応ノート
読み込み中…