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3-Chlorophenylacetic acid → 2-[(3-Chlorophenyl)acetamido)butyric acid iso-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chlorophenylacetic acid | HCID 15879 | — |
| 反応物 | Isobutyl 2-aminobutyrate | HCID 13743360 | — |
| 生成物 | 2-[(3-Chlorophenyl)acetamido)butyric acid iso-butyl ester | HCID 15547641 | — |
反応手順
Following General Procedure I′ above and using 3-chlorophenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure J′ above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure. NMR data was as follows:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06211235B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-2cb2eb909cf24a3f9208b26813f34f72 |
| 出典メモ | uspto-grants-2001_04 |