化工社化工社 化学情報印刷レポート · 研究参考用
Leucine methyl ester hydrochloride → N-[N-(Phenylacetyl)-L-alaninyl]-L-leucine Methyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Leucine methyl ester hydrochloride | HCID 2723695 | — |
| 反応物 | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| 生成物 | N-[N-(Phenylacetyl)-L-alaninyl]-L-leucine Methyl Ester | HCID 9923756 | — |
反応手順
Following General Procedure A and using N-(phenylacetyl)-L-alanine (from Example B1 above) and L-leucine methyl ester hydrochloride (Aldrich), the title compound was prepared as a solid (mp=102.5-105° C.). The reaction was monitored by tlc (Rf=0.25 in 50% EtOAc/hexanes).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06211235B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-7ff7abca63b649faafc14b1b9903e598 |
| 出典メモ | uspto-grants-2001_04 |