化工社化工社 化学情報印刷レポート · 研究参考用
4-Cyanobenzaldehyde → [4-(Aminomethyl)phenyl]methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Cyanobenzaldehyde | HCID 66042 | — |
| 反応物 | [3,5-Bis(benzyloxy)benzyl]amine hydrochloride | HCID 15505554 | — |
| 生成物 | [4-(Aminomethyl)phenyl]methanol | HCID 6496943 | 46% |
反応手順
This compound was prepared by reduction of 4-cyanobenzaldehyde according to the procedure described in preparation of 3,5-dibenzyloxybenzylamine. Yield was 46%: MP 102-123° C.; 1H NMR (Acetone-d6, 500 MHz) 7.27 (m, complex 4H), 4.58 (s, 2H), 3.72 (s, 2H), 3.69 (s, 1H) 2.77 (br, 1H), 2.45 (br, 1H);
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07427608B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-b108a33eb56d42ed8a2fc4baf57a0a48 |
| 出典メモ | uspto-grants-2008_09 |