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m-Formylbenzonitrile → [3-(Aminomethyl)phenyl]methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | m-Formylbenzonitrile | HCID 90670 | — |
| 反応物 | [3,5-Bis(benzyloxy)benzyl]amine hydrochloride | HCID 15505554 | — |
| 生成物 | [3-(Aminomethyl)phenyl]methanol | HCID 21880609 | 66% |
反応手順
This compound was prepared by reduction of 3-cyanobenzaldehyde according to the procedure described in preparation of 3,5-dibenzyloxybenzylamine. Yield was 66%: 1H NMR (Acetone-d6, 500 MHz) δ 7.32 (s, 1H), 7.23 (dd, 1H, J=7.6 and 7.0), 7.19, complex, 2H), 4.59 (s, 2H), 4.40 (s, 2H), 4.10 (br, 1H), 1.96 (br, 1H), 1.88 (br, 1H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07427608B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-b76b6ae21fe944ad8b04497ca70cb28e |
| 出典メモ | uspto-grants-2008_09 |