化工社化工社 化学情報印刷レポート · 研究参考用
Isopropanol → Baccatin III isopropanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isopropanol | HCID 3776 | — |
| 反応物 | Hexane | HCID 8058 | — |
| 反応物 | Baccatin Iii | HCID 65366 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Baccatin III isopropanol | HCID 86756610 | — |
反応手順
Baccatin III (100 mg, 0.17 mmol) was dissolved in dichloromethane (4 mL). Isopropanol was added (130 uL, 1000%), and the resulting solution was allowed to stir for 1 h. Hexane was added to the cloud point, and crystallization began. The baccatin III, 2-propanol complex (85 mg, 77%) was collected by filtration.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06215000B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-faa71747695648ada0aeab7e1000d413 |
| 出典メモ | uspto-grants-2001_04 |