化工社化工社 化学情報印刷レポート · 研究参考用
Hydrogen Peroxide → Perbenzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 反応物 | boric acid, sodium salt | HCID 159383 | — |
| 生成物 | Perbenzoic acid | HCID 523077 | — |
反応手順
m-Chloroperbenzoic acid (MCPBA), a mixture of sodium borate and trifluoroacetic acid or a mixture of acetic anhydride and H2O2 is preferably used for the oxidation. If desired, a commercially available wetting agent can additionally be added to the oxidizing agent. The reaction times lie in a wide range and range from about 0.5 to about 15 hours, preferably 1 to 8 hours. The reaction temperature ranges from −20 to about 100° C., preferably from 0 to about 85° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06215029B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-cf42e1c3c252406f96f3ed982b503b07 |
| 出典メモ | uspto-grants-2001_04 |