化工社化工社 化学情報印刷レポート · 研究参考用
Ioxynic acid → 2,6-Diiodo-4-(8-phenyloctylcarbamoyl)phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ioxynic acid | HCID 12065 | — |
| 反応物 | 8-Phenyloctan-1-amine | HCID 145556 | — |
| 生成物 | 2,6-Diiodo-4-(8-phenyloctylcarbamoyl)phenol | HCID 22237559 | — |
反応手順
The title compound was prepared as a solid (0.718 g, 66%) from 3,5-diiodo-4-hydroxybenzoic acid using 8-phenyloctylamine and a procedure similar to step 2 of Example 93; 1H NMR (DMSO-d6) δ1.17-1.36 (m, 8H), 1.41-1.61 (m, 4H), 2.48-2.60 (m, 2H), 3.20 (dd, J=5.9, 8.8 Hz, 2H), 7.10-7.21 (m, 3H), 7.21-7.30 (m, 2H), 8.21 (s, 2H), 8.40 (t, J=4.4 Hz, 1H), 10.06 (s, 1H); mass spectrum [(+) ESI], m/z 578 (M +H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06214877B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-f11b309d33c0464e85088f9906c90eb6 |
| 出典メモ | uspto-grants-2001_04 |