関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1-Butanol | HCID 263 | — |
| 反応物 | Iridium | HCID 23924 | — |
| 反応物 | Tantalum | HCID 23956 | — |
| 触媒 | Titanium | HCID 23963 | — |
| 生成物 | HCID 178514811 | HCID 178514811 | — |
反応手順
After the roughened titanium substrate surface was heat treated, it was painted with a n-butanol solution containing salts of iridium and tantalum. The ratio of iridium to tantalum in the solution was about 65% to 35% by weight. The solution was allowed to dry at ambient temperature for approximately 20 minutes. The painted titanium substrate was subsequently heat treated in a furnace having an oxygen containing atmosphere at approximately 500° C. for approximately 20-30 minutes to form an iridium oxide/tantalum oxide composite coating. The process of painting and heat treating the titanium substrate was repeated to obtain a first layer having a total loading of 2.0 g/m2. After the desired loading was achieved, the anode was heat treated for approximately one hour at approximately 500° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06217729B1 |
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| 出典データセット | uspto-grants-2001_04 |
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| ORD ID | ord-c7848c10c67f4658b8f52f05a07d6b97 |
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| 出典メモ | uspto-grants-2001_04 |
|---|