HCID 67483482、化合物 → HCID 54185295、化合物
反応式
[CH:1]([C:4]1[C:9]([C:10](OCC)=[O:11])=[C:8]([C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([F:21])[CH:16]=2)[C:7]([CH:22]=[CH:23][CH2:24][CH2:25][CH3:26])=[C:6]([CH:27]([CH3:29])[CH3:28])[N:5]=1)([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCC>[CH:1]([C:4]1[C:9]([CH2:10][OH:11])=[C:8]([C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([F:21])[CH:16]=2)[C:7]([CH:22]=[CH:23][CH2:24][CH2:25][CH3:26])=[C:6]([CH:27]([CH3:28])[CH3:29])[N:5]=1)([CH3:3])[CH3:2]参加物
3
実験手順
The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefin isomers): δ 0.78 (m, 3 H), 1.13-1.37 (m, 14 H), 1.93 (m, 2 H), 3.41 (m, 2 H), 4.40 (s, 2 H), 5.28-5.45 (m, 1 H), 6.0 (m, 1 H), 6.87-7.07 (m, 3 H), 7.34 (m, 1 H). Rf=0.36 (10% ethyl acetate/n-hexane). mp 117-118° C.
出典と根拠
- ORDレコード
- ord-d684e8ac5fa74398b0a5111d766d8914
- 出典データセット
- uspto-grants-2001_04