化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 3-(Chloromethyl)-1,1'-biphenyl
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-Biphenylmethanol | HCID 603556 | — |
| 生成物 | 3-(Chloromethyl)-1,1'-biphenyl | HCID 15480892 | — |
反応手順
A solution of 50 mg of 3-hydroxymethylbiphenyl in 1.5 mL thionyl chloride was heated at reflux temperature for 4 hr, cooled to room temperature and the solvent removed by evaporation under reduced pressure to yield 45 mg of 3-chloromethylbiphenyl which was used in the next step without further purification or characterization.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06221871B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-9e13e4c29c3e404eb17e55021b1c95f0 |
| 出典メモ | uspto-grants-2001_04 |