化工社化工社 化学情報印刷レポート · 研究参考用
Aniline → Benzeneethanamine, N-phenyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Styrene | HCID 7501 | — |
| 溶媒 | Ethyl acetate hexane | HCID 21226206 | — |
| 生成物 | Benzeneethanamine, N-phenyl- | HCID 74443 | 78% |
反応手順
According to GWM, 0.011 mol (=1.00 ml) of aniline and 0.011 mol (=1.25 ml) of styrene are reacted with one another. The product is isolated by column chromatography using ethyl acetate/n-hexane (1:3) as eluent, the product N-phenylethylaniline being obtained as a yellow liquid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06222073B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-cde6fc26c17d47a3be4c2061a84b856f |
| 出典メモ | uspto-grants-2001_04 |