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Adipic Acid → Epoxide resin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Adipic Acid | HCID 196 | — |
| 反応物 | 1-Phenylimidazole | HCID 81595 | — |
| 反応物 | 2,4-Imidazolidinedione, 5,5-dimethyl-1,3-bis(2-oxiranylmethyl)- | HCID 85828 | — |
| 生成物 | Epoxide resin | HCID 16213861 | — |
反応手順
Adipic acid (73 g) is added in portions with stirring to N,N'-diglycidyl-5,5-dimethylhydantoin (8.04 epoxide equiv./kg, 200 g) containing N-phenylimidazole (0.4 g), the temperature is kept at 100° C. and the addition is carried out over 40 minutes. The heating is maintained at 100° C. for a further 41/3 hours by which time the epoxide content has fallen to 2.35 equiv./kg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04440802 |
| 出典データセット | uspto-grants-1984_04 |
| ORD ID | ord-d2319419150b42f5927fc8cca666e4f5 |
| 出典メモ | uspto-grants-1984_04 |