Benzylamine → N-benzyl-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine

HRID 32561ノート

反応式

HRID 32561 の反応式
CO[C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1OC)[CH2:6][N:7]=[CH:8][C:9]1[S:17][C:12]2[N:13]=[CH:14][N:15]=[CH:16][C:11]=2[CH:10]=1.C(N)C1C=CC=CC=1>>[CH2:6]([N:7]=[CH:8][C:9]1[S:17][C:12]2[N:13]=[CH:14][N:15]=[CH:16][C:11]=2[CH:10]=1)[C:5]1[CH:4]=[CH:3][CH:20]=[CH:19][CH:18]=1

参加物

3

反応物 2

HCID 7504BenzylamineHCID 17965764N-(3,4-dimethoxybenzyl)-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine

生成物 1

HCID 69194866N-benzyl-N-[thieno[2,3-d]pyrimidin-6-ylmethylidene]amine

実験手順

The title compound was prepared by a similar process to that described for Intermediate 14 but using benzylamine in place of 3,4-dimethoxybenzylamine. Pale yellow solid (69 mg, 100%), which was used directly without further purification.

後処理

  1. customPale yellow solid (69 mg, 100%), which was used directly without further purification

出典と根拠

ORDレコード
ord-380526473e64476f96944287284f4188
出典データセット
uspto-grants-2008_09
特許番号
US07427616B2

反応ノート

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