関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Enoxacin hydrochloride | HCID 12901163 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Enoxacin | HCID 3229 | — |
反応手順
About 10 g of AT-2266.hydrochloride was dissolved to hot water (about 70° C.) and the solution was neutralized with 15% aqueous solution of sodium hydroxide which was warmed to 70° C. previously. The precipitate was collected by filtration and dried at 70° to 80° C. for elimination of adhering water to give the AT-2266.sesquihydrate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04442101 |
|---|
| 出典データセット | uspto-grants-1984_04 |
|---|
| ORD ID | ord-b477c5e573b74f0f821d8fb612284fb3 |
|---|
| 出典メモ | uspto-grants-1984_04 |
|---|
