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2-Propenoic acid, 3-phenyl- → Europium(3+);tris(3-phenylprop-2-enoate)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Europium chloride, anhydrous 99.9% | HCID 9859933 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Europium(3+);tris(3-phenylprop-2-enoate) | HCID 86739358 | — |
反応手順
Then a sodium cinnamate aqueous solution obtained in advance by dissolving 1.64 g of sodium hydroxide in 300 ml of purified water and thereafter dissolving 6.06 g of cinnamic acid (purity 99.9%, conjugate number 4) thoroughly in the resultant solution was gradually added with continued stirring into the aforementioned aqueous europium chloride solution. Consequently, a white salt of europium cinnamate was produced in the form of a precipitate. Thereafter, the reaction solution was adjusted to pH 6.5 with a 0.1 N sodium hydroxide aqueous solution added under thorough stirring.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04443380 |
| 出典データセット | uspto-grants-1984_04 |
| ORD ID | ord-3ed6da98ea004559a8413aa47f486281 |
| 出典メモ | uspto-grants-1984_04 |