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2-Propenoic acid, 3-phenyl- → Lanthanum(3+);tris(3-phenylprop-2-enoate)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Lanthanum(III)chloride | HCID 9859665 | — |
| 反応物 | Europium chloride, anhydrous 99.9% | HCID 9859933 | — |
| 生成物 | Lanthanum(3+);tris(3-phenylprop-2-enoate) | HCID 86739359 | — |
反応手順
Europium cinnamate, [(C6H5CH=CHCOO)3Eu], was obtained by following the procedure of Comparative Example 4, except that the quantity of sodium hydroxide was changed from 1.698 g to 1.132 g, the quantity of cinnamic acid was changed from 6.289 g to 4.193 g and 5.0 g of lanthanum chloride was substituted by 3.456 g of europium chloride (EuCl3.6H2O; purity 99.9%). Then, the total quantity of lanthanum cinnamate obtained as described in Comparative Example 4 and the total quantity of europium cinnamate described above were placed in an agate mortar and thoroughly mixed until a homogeneous mixture was obtained. Consequently, there was obtained a physical mixture of 0.6 lanthanum cinnamate and 0.4 europium cinnamate;
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04443380 |
| 出典データセット | uspto-grants-1984_04 |
| ORD ID | ord-2bbee65729554e2a892fecef50b0931d |
| 出典メモ | uspto-grants-1984_04 |