2-Ethylbutyraldehyde → 3,7-Diethyl-5-azanona-3,5-diene

HRID 325979

反応式

HRID 325979 の反応式
[OH-].[NH4+:2].[CH2:3]([CH:5]([CH2:8][CH3:9])[CH:6]=O)[CH3:4]>>[CH2:3]([C:5](=[CH:6][N:2]=[CH:6][CH:5]([CH2:8][CH3:9])[CH2:3][CH3:4])[CH2:8][CH3:9])[CH3:4]

参加物

3

反応物 2

HCID 73592-EthylbutyraldehydeHCID 14923Ammonium Hydroxide

生成物 1

HCID 124134703,7-Diethyl-5-azanona-3,5-diene収率 76.5%

実験手順

To a sample of 250 grams of 28% ammonium hydroxide was added 215 grams of 2-ethylbutyraldehyde and the heterogeneous mixture was stirred for 18 hours at ambient temperature. The resulting organic layer was separated, and after drying, slowly distilled at atmospheric pressure to yield 148.8 grams of 3,7-diethyl-5-azanona-3,5-diene.

後処理

  1. customThe resulting organic layer was separated
  2. customafter drying
  3. distillationslowly distilled at atmospheric pressure

出典と根拠

ORDレコード
ord-7485e4e1d9c24c839b4ca499287abe82
出典データセット
uspto-grants-1984_04
特許番号
US04443609

関連ノート

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