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2,2,6,6-Tetramethyl-4-piperidone → N-(2,2,6,6-tetramethyl-4-piperidyl)-3-morpholinopropylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,2,6,6-Tetramethyl-4-piperidone | HCID 13220 | — |
| 反応物 | N-(3-Aminopropyl)morpholine | HCID 61055 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | N-(2,2,6,6-tetramethyl-4-piperidyl)-3-morpholinopropylamine | HCID 19736767 | — |
反応手順
288.4 g (2 mol) of 3-morpholinopropylamine, 310.5 g (2 mol) of 2,2,6,6-tetramethyl-4-piperidone and 300 ml of methanol are introduced into a 2 litre autoclave; 15 g of 5% Pt-on-carbon are added, and hydrogenation is carried out at 60 bar and 60° C. until the absorption of hydrogen ceases (about 15 hours).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05268401 |
| 出典データセット | uspto-grants-1993_12 |
| ORD ID | ord-da77c7797a634342bdc5c8cedae7aaa1 |
| 出典メモ | uspto-grants-1993_12 |