1-Propanone, 3-(dimethylamino)-1-phenyl-, hydrochloride (1:1) → 3-(Dimethylamino)-1-phenyl-1-propanone
反応式
Cl.[CH3:2][N:3]([CH3:14])[CH2:4][CH2:5][C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:7].C(=O)(O)[O-].[Na+]>ClCCl>[CH3:14][N:3]([CH3:2])[CH2:4][CH2:5][C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:7]参加物
4
実験手順
3-Dimethylaminopropiophenone hydrochloride (20 g) was treated with aqueous sodium bicarbonate solution in dichloromethane. The layers were separated and the organic phase was dried over anhydrous magnesium sulfate, filtered, and the filtrate was evaporated to provide 15.8 g of 3-dimethylaminopropiophenone.
後処理
- customThe layers were separated
- dry with materialthe organic phase was dried over anhydrous magnesium sulfate
- filtrationfiltered
- customthe filtrate was evaporated
出典と根拠
- ORDレコード
- ord-8405d6c06e7a480280c47c4f322f1fd8
- 出典データセット
- uspto-grants-1993_12
- 特許番号
- US05268468
反応ノート
読み込み中…