関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sodium Phosphate, Dibasic | HCID 24203 | — |
| 反応物 | Chloro hypochlorite;zirconium | HCID 71304769 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Zirconium phosphate | HCID 160986 | 123.4% |
反応手順
Zirconium oxychloride (ZrOCl2.8H2O) 36.1 g (0.112 mole) was dissolved in 50 ml of water, and to the resulting solution was added 200 ml of an aqueous solution containing disodium hydrogenphosphate (Na2HPO4) 31.8 g (0.224 mole) to form a white precipitate. The resulting mixture was stirred at 80° C. for one hour, and the white precipitate was sufficiently washed with water by a decantation method, filtered, further washed with water, and dried at 120° C. to obtain zirconium phosphate (Zr(HPO4)2) 30.1 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05268503 |
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| 出典データセット | uspto-grants-1993_12 |
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| ORD ID | ord-b5d270aad2eb41ab9c5ad63e16bdecb0 |
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| 出典メモ | uspto-grants-1993_12 |
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