化工社化工社 化学情報印刷レポート · 研究参考用
Cyclopropanemethanamine → 2-Chloro-5-(cyclopropylmethyl-sulfamoyl)-benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclopropanemethanamine | HCID 75646 | — |
| 反応物 | Benzoic acid, 2-chloro-5-[(methylamino)sulfonyl]- | HCID 111724 | — |
| 反応物 | 2-Chloro-5-sulfino-benzoic acid | HCID 15112904 | — |
| 生成物 | 2-Chloro-5-(cyclopropylmethyl-sulfamoyl)-benzoic acid | HCID 29035580 | 81% |
反応手順
The title compound was synthesised according to the procedure described for 2-Chloro-5-methylsulfamoyl-benzoic acid from 2-Chloro-5-sulfino-benzoic acid and cyclopropylmethylamine and obtained in 81% yield. MS (m/e): 288.0 (MH−, 100%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07427612B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-fc1203deeb0949a888ece709f3315086 |
| 出典メモ | uspto-grants-2008_09 |