Ammonia → 2-(4-Methoxyphenoxy)ethanimidamide
反応式
[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6]([O:7][CH2:8][C:9](=[NH:12])OC)=[CH:5][CH:4]=1.[NH3:15]>C(O)C>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([O:7][CH2:8][C:9]([NH2:12])=[NH:15])=[CH:13][CH:14]=1参加物
4
実験手順
23.9 g (0.122 mole) of methyl 2-(4-methoxyphenoxy)acetimidate are added to a solution, maintained at 10° C., of 10.4 g (0.61 mole) of ammonia in 480 ml of absolute ethanol. The reaction mixture is left for 2 days at room temperature and the excess ammonia is then driven off with a stream of nitrogen. The solution obtained is used in the next step without further purification.
後処理
- customThe solution obtained
- customis used in the next step without further purification
出典と根拠
- ORDレコード
- ord-83bc569192db41a28229e94f15f4fcf6
- 出典データセット
- uspto-grants-1993_12
- 特許番号
- US05270465
反応ノート
読み込み中…