関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Calcium Acetate | HCID 6116 | — |
| 反応物 | 3-(1-Dodecen-1-yl)dihydro-2,5-furandione | HCID 32933 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | Calcium dodecenyl succinate | HCID 86747412 | 113.2% |
反応手順
A solution of 313.5 g (1.98 mol) calcium acetate in 1000 ml water was added to a solution of 570 g (1.98 mol) dodecenyl succinic anhydride in 1000 ml isopropanol. The mixture was then heated to 90° C., left at that temperature for 1.5 h and then concentrated in a water jet vacuum. The residue was dried in vacuo in a drying cabinet at 100° C. 680 g of the calcium soap were obtained in the form of a colorless powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05271855 |
|---|
| 出典データセット | uspto-grants-1993_12 |
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| ORD ID | ord-93f2ffbeba514eb389fbfa7f33845a47 |
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| 出典メモ | uspto-grants-1993_12 |
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