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HRID 32697作成日：2026年10月25日

Benzoic acid, 2-chloro-5-[(methylamino)sulfonyl]- → 3-[4-(4-Acetyl-2-fluoro-phenyl)-piperazine-1-carbonyl]-4-chloro-N-methyl-benzenesulfonamide

https://huagongshe.com/reaction/32697

反応式

関与物質

役割名称HCID仕込み量
反応物Benzoic acid, 2-chloro-5-[(methylamino)sulfonyl]-HCID 111724—
反応物1-(3-Fluoro-4-piperazin-1-ylphenyl)ethanoneHCID 685610—
生成物3-[4-(4-Acetyl-2-fluoro-phenyl)-piperazine-1-carbonyl]-4-chloro-N-methyl-benzenesulfonamideHCID 59793606—

反応手順

The title compound was prepared according to the procedure described for example K/step2 from 1-(3-Fluoro-4-piperazin-1-yl-phenyl)-ethanone and 2-Chloro-5-methylsulfamoyl-benzoic acid (CAS: 68901-09-7; BE 620741) (69%, light yellow foam, MS (m/e): 452.1 (M−H, 100%)

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07427612B2
出典データセットuspto-grants-2008_09
ORD IDord-542cc5d85d9f4f798bb5d75035cf9873
出典メモuspto-grants-2008_09