化工社化工社 化学情報印刷レポート · 研究参考用
Morpholine → 5-Bromo-2-morpholin-yl-benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Morpholine | HCID 8083 | — |
| 反応物 | 5-Bromo-2-fluorobenzoic acid | HCID 2736315 | — |
| 生成物 | 5-Bromo-2-morpholin-yl-benzoic acid | HCID 59793690 | — |
反応手順
The title compound was prepared according to the procedure described for example B step 1 from 5-Bromo-2-fluorobenzoic acid and morpholine except that the mixture was heated at 130° C. for 48 hours (77%, white solid), 1-H-NMR (300 MHz, CDCl3) δ=8.45 (d), 7.74 (dxd, 7.33 (d)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07427612B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-cccc6f14661d481989037573119dc89c |
| 出典メモ | uspto-grants-2008_09 |