化工社化工社 化学情報印刷レポート · 研究参考用
11-Bromoundecanoic acid → Undecanoyl chloride, 11-bromo-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 11-Bromoundecanoic acid | HCID 17812 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | Undecanoyl chloride, 11-bromo- | HCID 85202 | — |
反応手順
11-Bromoundecanoic acid (400 g) was added to thionyl chloride (600 ml) and the solution heated at 80° for 0.5 hour. The thionyl chloride was distilled off and the dark oily residue distilled in vacuo to give 11-bromoundecanoyl chloride, b.p. 144°, 0.7 mm Hg, (346.8 g, 81%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05273740 |
| 出典データセット | uspto-grants-1993_12 |
| ORD ID | ord-6cf0c1ec3405470791493e943ea7bff2 |
| 出典メモ | uspto-grants-1993_12 |