関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | 2,6-Dichloro-3-nitrotoluene | HCID 97155 | — |
| 生成物 | 3-Chloro-2-methyl-6-nitroaniline | HCID 12953020 | 76% |
反応手順
A suspension of 2,6-dichloro-3-nitrotoluene (6.0 g, 29 mmol) in 50% methanolic ammonia (60 mL) was stirred at 130° C. (340 lb pressure) for 18 hours. The autoclave was cooled to -30° C., opened, and the precipitate was filtered off and washed with methanol to give 4.14 g (76%) of 3-chloro-2-methyl-6-nitrobenzenamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05273975 |
|---|
| 出典データセット | uspto-grants-1993_12 |
|---|
| ORD ID | ord-6a783ee54f534c5382fab3da4c85a8fe |
|---|
| 出典メモ | uspto-grants-1993_12 |
|---|
