HCID 19108500、化合物 → 5-((Phenylmethyl)methylamino)-5,6-dihydro-4H-imidazo(4,5,1-ij)quinolin-2(1H)-one

HRID 327469

反応式

HRID 327469 の反応式
[NH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:11]=1[NH:10][CH2:9][CH:8]([NH:12][C:13](=O)OC(C)(C)C)[CH2:7]2.[CH3:20][OH:21].CCO[CH2:25][CH3:26]>>[C:25]1([CH2:26][N:12]([CH3:13])[CH:8]2[CH2:7][C:6]3[C:11]4=[C:2]([NH:1][C:20](=[O:21])[N:10]4[CH2:9]2)[CH:3]=[CH:4][CH:5]=3)[CH:4]=[CH:3][CH:2]=[CH:11][CH:6]=1

参加物

3

反応物 2

HCID 19108500HCID 19108500、化合物HCID 21864698Diethyl ether methanol

生成物 1

HCID 199194845-((Phenylmethyl)methylamino)-5,6-dihydro-4H-imidazo(4,5,1-ij)quinolin-2(1H)-one

実験手順

This compound was prepared by following the procedure of Example 44 part B, but substituting 1,2,3,4-tetrahydro-N3 -methyl-N3 -(phenylmethyl)quinoline-3,8-diamine for t-butyl (8-amino-1,2,3,4-tetrahydro-3-quinolyl)carbamate. The bulk of the product was converted to the hydrochloride salt, mp 145°-149° C. from methanol/ether.

後処理

  1. customThis compound was prepared

出典と根拠

ORDレコード
ord-3991cfb075cb44c49d2dbd97276a8696
出典データセット
uspto-grants-1993_12
特許番号
US05273975

関連ノート

読み込み中…