化工社化工社 化学情報印刷レポート · 研究参考用
2-(2,4-Dichlorophenoxy)ethanol → 2-(2,4-Dichlorophenoxy)ethanol sulfamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(2,4-Dichlorophenoxy)ethanol | HCID 8444 | — |
| 反応物 | Chlorosulfamic acid | HCID 24499 | — |
| 生成物 | 2-(2,4-Dichlorophenoxy)ethanol sulfamate | HCID 19108689 | — |
反応手順
The title compound was prepared by the procedures of Example 33 from sulfamoyl chloride and 2-(2,4-dichlorophenoxy)ethanol. The viscous oil obtained solidified and was recrystallized from isopropyl ether to give the solid title compound, mp 75°-77° C., in 35% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05273993 |
| 出典データセット | uspto-grants-1993_12 |
| ORD ID | ord-1dee74034a374557bd1fb843cefa570e |
| 出典メモ | uspto-grants-1993_12 |