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2,6-Dichlorophenol → 2,6-Dichlorophenyl sulfamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dichlorophenol | HCID 6899 | — |
| 反応物 | Chlorosulfonyl isocyanate | HCID 70918 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2,6-Dichlorophenyl sulfamate | HCID 19018467 | 71.5% |
反応手順
This compound was prepared according to the procedure of Example 84 from a mixture of 16.3 g (0.10 mole) of 2,6-dichlorophenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 75 ml of toluene to obtain 17.3 g (71%) of the title compound after recrystallization from benzene, mp 114.5°-116° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05273993 |
| 出典データセット | uspto-grants-1993_12 |
| ORD ID | ord-070acc2ffaec4b4b8315fc08af0f948c |
| 出典メモ | uspto-grants-1993_12 |