化工社化工社 化学情報印刷レポート · 研究参考用
Water → Trans-phenylpropylene oxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | trans-beta-METHYLSTYRENE | HCID 252325 | — |
| 生成物 | Benzaldehyde | HCID 240 | 14% |
| 生成物 | Trans-phenylpropylene oxide | HCID 123339 | 86% |
反応手順
The metal-catalyzed epoxidation of trans-β-methylstyrene was performed as described in Example 2 with the substitution of Co(OAc)2. 4 H2O (where OAc=acetate) (0.0058 g, 2.3×10-5 moles) as the catalyst. After 16 hours of reaction, the complete oxidation of the substrate produced benzaldehyde (14%) and 1-phenylpropylene oxide (86%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05274139 |
| 出典データセット | uspto-grants-1993_12 |
| ORD ID | ord-1124b1086ea74b099e9de1b9985c1c60 |
| 出典メモ | uspto-grants-1993_12 |