化工社化工社 化学情報印刷レポート · 研究参考用
5-Bromopentyl acetate → (E)-3-[2-[[5-(Acetyloxy)pentyl]oxy]-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic Acid Methyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Bromopentyl acetate | HCID 85140 | — |
| 反応物 | (E)-3-[2-Hydroxy-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic Acid Methyl Ester | HCID 67780365 | — |
| 生成物 | (E)-3-[2-[[5-(Acetyloxy)pentyl]oxy]-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic Acid Methyl Ester | HCID 67780134 | 77% |
反応手順
Using the procedure of example 63, (E)-3-[2-hydroxy-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic acid methyl ester from the preceding example was converted into the title compound by alkylation with 5-bromopentylacetate. The product was obtained as a colorless oil in 77% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05273999 |
| 出典データセット | uspto-grants-1993_12 |
| ORD ID | ord-03d2ce19dc984a52b0d1775b100668d0 |
| 出典メモ | uspto-grants-1993_12 |