HCID 70637584、化合物 → HCID 70637164、化合物
反応式
[C:1]([CH:3]1[CH2:21][CH2:20][N:6]2[C:7]3[CH:19]=[CH:18][CH:17]=[CH:16][C:8]=3[CH2:9][C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=3[CH:5]2[CH2:4]1)#[N:2]>O>[NH2:2][CH2:1][CH:3]1[CH2:21][CH2:20][N:6]2[C:7]3[CH:19]=[CH:18][CH:17]=[CH:16][C:8]=3[CH2:9][C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=3[CH:5]2[CH2:4]1参加物
3
試薬・触媒・溶媒 1
実験手順
3 g of 2-cyano-1,2,3,4,10,14b-hexahydro-pyridino[1,2-a]-dibenzo[c,f]-azepine (ax.), is dissolved in 27 ml of concentrated H2S04 and 0.3 ml of water. The solution is heated at a steambath for about 2 hours. The reaction mixture is then poured into 500 ml of water, whereupon the aqueous mixture obtained is extracted into ether.
後処理
- temperatureThe solution is heated at a steambath for about 2 hours
- customobtained
- extractionis extracted into ether
出典と根拠
- ORDレコード
- ord-6e7f10cecef146dd973edbc17d0b643e
- 出典データセット
- uspto-grants-1977_04
- 特許番号
- US04016161
反応ノート
読み込み中…