化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Epoxybutane → 1-(p-Ethylphenoxy)-butan-2-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Epoxybutane | HCID 7834 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 4-Ethylphenol | HCID 31242 | — |
| 生成物 | 1-(p-Ethylphenoxy)-butan-2-ol | HCID 21444115 | 76.3% |
反応手順
In a closed vessel 12.2g (0.1 mol) of p-ethylphenol, 7.2 g (0.1 mol) of 1,2-butylene oxide and 0.8 ml of a 50% aqueous solution of sodium hydroxide were heated at 140° to 145° C for 4 hours in the same way as in Example 1. The reaction mixture obtained was treated in the same way as in Example 1 to afford 14.8 g of 1-(p-ethylphenoxy)-butan-2-ol (compound No. 52) in a yield of 76.3%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04016186 |
| 出典データセット | uspto-grants-1977_04 |
| ORD ID | ord-92c1464e53d14e5f99903d078d027c3e |
| 出典メモ | uspto-grants-1977_04 |