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HRID 328151作成日:2026年10月24日

1,2-Epoxybutane → 1-(p-Ethylphenoxy)-butan-2-ol

https://huagongshe.com/ja/reaction/328151

反応式

関与物質

役割名称HCID仕込み量
反応物1,2-EpoxybutaneHCID 7834—
反応物Sodium HydroxideHCID 14798—
反応物4-EthylphenolHCID 31242—
生成物1-(p-Ethylphenoxy)-butan-2-olHCID 2144411576.3%

反応手順

In a closed vessel 12.2g (0.1 mol) of p-ethylphenol, 7.2 g (0.1 mol) of 1,2-butylene oxide and 0.8 ml of a 50% aqueous solution of sodium hydroxide were heated at 140° to 145° C for 4 hours in the same way as in Example 1. The reaction mixture obtained was treated in the same way as in Example 1 to afford 14.8 g of 1-(p-ethylphenoxy)-butan-2-ol (compound No. 52) in a yield of 76.3%.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04016186
出典データセットuspto-grants-1977_04
ORD IDord-92c1464e53d14e5f99903d078d027c3e
出典メモuspto-grants-1977_04