N,N-Bis(2-hydroxyethyl)benzamide → N,N-bis(2-oleoyloxyethyl)benzamide

HRID 328429

反応式

HRID 328429 の反応式
[OH:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][OH:15])[C:5](=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[C:16](Cl)(=[O:34])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]/[CH:24]=[CH:25]\[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33]>>[C:16]([O:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][O:15][C:16](=[O:34])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]/[CH:24]=[CH:25]\[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33])[C:5](=[O:12])[C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1)(=[O:34])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]/[CH:24]=[CH:25]\[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33]

参加物

3

反応物 2

HCID 94109N,N-Bis(2-hydroxyethyl)benzamideHCID 5364783Oleoyl chloride

生成物 1

HCID 54601942N,N-bis(2-oleoyloxyethyl)benzamide

実験手順

N,N-bis(oleoyloxyethyl)benzamide was prepared by the procedue of example 1 from 19.5 gms. (0.1 mole) of N,N-bis(2-hydroxyethyl)benzamide and 60 gms. (0.2 mole) of oleoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

後処理

  1. customN,N-bis(oleoyloxyethyl)benzamide was prepared by the procedue of example 1 from 19.5 gms

出典と根拠

ORDレコード
ord-4b445f1cc0134412920a680cbbb6d117
出典データセット
uspto-grants-1977_04
特許番号
US04017522

関連ノート

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