N,N-Bis(2-hydroxyethyl)benzamide → N,N-bis(2-erucoyloxyethyl)benzamide

HRID 328430

反応式

HRID 328430 の反応式
[OH:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][OH:15])[C:5](=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[C:16](Cl)(=[O:38])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]/[CH:28]=[CH:29]\[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37]>>[C:16]([O:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][O:15][C:16](=[O:38])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]/[CH:28]=[CH:29]\[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])[C:5](=[O:12])[C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1)(=[O:38])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]/[CH:28]=[CH:29]\[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37]

参加物

3

反応物 2

HCID 94109N,N-Bis(2-hydroxyethyl)benzamideHCID 5364502Erucoyl chloride

生成物 1

HCID 54598631N,N-bis(2-erucoyloxyethyl)benzamide

実験手順

N,N-bis(2-erucoyloxyethyl)benzamid was prepared by the procedure of example 1 from 19.5 gms. (0.1 mole) of N,N-bis(2-hydroxyethyl)benzamide and 71 gms. (0.2 mole) of erucoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

後処理

  1. customN,N-bis(2-erucoyloxyethyl)benzamid was prepared by the procedure of example 1 from 19.5 gms

出典と根拠

ORDレコード
ord-7c54b5e1adc2457296b177b2a1af74e6
出典データセット
uspto-grants-1977_04
特許番号
US04017522

関連ノート

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