Oleoyl chloride → N-methyl-N-(2-oleoyloxyethyl)-p-toluamide

HRID 328444

反応式

HRID 328444 の反応式
[CH3:1][N:2]([CH2:12][CH2:13][OH:14])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4].[C:15](Cl)(=[O:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32]>>[CH3:1][N:2]([CH2:12][CH2:13][O:14][C:15](=[O:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4]

参加物

3

反応物 2

HCID 5364783Oleoyl chlorideHCID 21441887N-(2-hydroxyethyl)-N,4-dimethylbenzamide

生成物 1

HCID 68123309N-methyl-N-(2-oleoyloxyethyl)-p-toluamide

実験手順

N-methyl-N-(2-oleoyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)-p-toluamide and 30 gms. (0.1 mole) of oleoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

後処理

  1. customN-methyl-N-(2-oleoyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms

出典と根拠

ORDレコード
ord-af13e5383dc24d6e8fc9b3614a7f2665
出典データセット
uspto-grants-1977_04
特許番号
US04017522

関連ノート

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