関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Beta-Alanine | HCID 239 | — |
| 反応物 | Magnesium Carbonate | HCID 11029 | — |
| 反応物 | Hypobromous acid | HCID 83547 | — |
| 反応物 | Aluminiumato(2-) sulfamatato(2-) sulfurimidatato(2-)--sulfamato(2-) (1/1/1/1) | HCID 21989125 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Magnesium beta-alaninate | HCID 86734646 | — |
反応手順
Magnesium β-alaninate was prepared by reacting 4.86 grams of β-alanine with 2.5 grams of basic magnesium carbonate (26.3% Mg) in 25 grams of water. The mixture was heated at 75° C. with agitation for one half hour. The hot solution was added to 100 grams of zirconyl hydroxybromide solution (17.5% Zr). To the resultant solution was added 14.2 grams of 2/3 basic aluminum sulfamate, Al(OH)2 (OSO2NH2) (9.19% Al, see U.S. Pat. No. 2,765,213 by S. M. Beekman) with agitation. The solution was evaporated at 60° C. under a vacuum of 252 m of Hg. The product contained 1.8% Al, 30.9% Zr, 0.53 Mg, 5.91% β-alanine and 5.3% sulfamates.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04017599 |
|---|
| 出典データセット | uspto-grants-1977_04 |
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| ORD ID | ord-c6d8b3a5792f42c789ae2ac50ddf562d |
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| 出典メモ | uspto-grants-1977_04 |
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