関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Aluminum Hydroxide | HCID 10176082 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Aluminum Sulfate | HCID 24850 | — |
反応手順
Separately, 2.12 kg of 98% conc. sulfuric acid and 1 liter of water were added to 1 kg of the same aluminum hydroxide as set forth above, and the mixture was heated at 100° C. to form a solution. Then, water was added to form 3 liters of an aqueous solution of aluminum sulfate. The resulting sodium aluminate solution and the resulting aluminum sulfate solution were separately added dropwise over the course of 1 hour to 7 liters of water being stirred, while maintaining the pH of the mixture at 8.5 to 9.0. The reaction mixture was aged for 1 hour, and then, nitric acid was added to the solution to adjust its pH to 6.0. The resulting aluminum hydroxide was filtered, washed with water, and dried at 150° C. to form boehmite-like aluminum oxide monohydrate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04018706 |
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| 出典データセット | uspto-grants-1977_04 |
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| ORD ID | ord-03d19432eb914a37ae285835a8f425da |
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| 出典メモ | uspto-grants-1977_04 |
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