4,4-Difluoro-1-keto-2-trifluoromethyl-1,4-dihydronaphthalene → 2,3,5,6-Tetramethylphenol

HRID 329245

反応式

HRID 329245 の反応式
F[C:2]1(F)[C:11]2[C:6](=[CH:7]C=C[CH:10]=2)[C:5](=[O:12])[C:4]([C:13](F)(F)F)=[CH:3]1.F[C:19]1(F)C2C(=CC=CC=2)C(F)(F)C=C1C(F)(F)F>CC(C)=O>[CH3:13][C:4]1[C:3]([CH3:19])=[CH:2][C:11]([CH3:10])=[C:6]([CH3:7])[C:5]=1[OH:12]

参加物

4

反応物 2

HCID 214392094,4-Difluoro-1-keto-2-trifluoromethyl-1,4-dihydronaphthaleneHCID 21439217HCID 21439217、化合物

生成物 1

HCID 106942,3,5,6-Tetramethylphenol

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

Anal. Calcd. for C30H39F3OS2 : C, 67.16; H, 7.28; F, 10.63; S, 11.94. Found (A): C, 63.64; H, 5.37; F, 12.85; S, 7.69; MW, 2737; Found (B): C, 67.62; H, 5.37; F, 11.62; S, 11.80; MW, 5785; Found (C); C, 65.00; H, 5.72; F, 12.61; S, 12.98; MW, 928;

出典と根拠

ORDレコード
ord-7bb1e470b575490d82da319b8c669e2d
出典データセット
uspto-grants-1977_04
特許番号
US04020112

関連ノート

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